So, I changed the barrel today. The cold trap was still full of liquid nitrogen so we had to take that off and put the other one on. When you have a cold trap in a machine under vacuum nothing condenses on the outside, but when you bring that machine up to atmospheric pressure, water from the air freezes to the cold trap almost immediately. The outside of the trap gets really really cold and we have to use special gloves to hold it. I didn't get any pictures of removing the trap, but here's a picture of it just afterwards.
Here's a photo of the trap after a few more minutes.
It's got a few millimeters of frost on it at this point. You can see a bit of nitrogen still steaming near the bottom and out of the top.
Early night home tonight....leaving at 9pm! woo hoo!!! Although, this early night is also the end of 60 hours in the lab.....sooooo.....not that early.
That's all for now. See you tomorrow, hopefully with all my new ages collected!
1 comment:
Love your blog!!!
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